• J. Forensic Sci. · Jan 1998

    Determining sodium azide concentration in blood by ion chromatography.

    • R Kruszyna, R P Smith, and H Kruszyna.
    • Department of Pharmacology and Toxicology, Dartmouth Medical School, Hanover, New Hampshire, USA.
    • J. Forensic Sci. 1998 Jan 1; 43 (1): 200-2.

    AbstractWe describe a simple method for measuring sodium azide concentrations in aliquots of blood and other tissues. Aliquots are acidified, converting azide to volatile hydrazoic acid (HN3) which is then trapped in sodium hydroxide. We analyze the resulting aliquots by ion chromatography, using a sodium tetraborate eluent and suppressed conductivity detection. The method is sensitive to at least 100 ng/mL.

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